Pengaruh Konsentrasi Doping Zn2+ Terhadap Nilai Konstanta Optik Nanopartikel Mn1-xZnxFe2O4
I Putu Tedy Indrayana, Rachmad Almi Putra
Kata Kunci:
Zn2 doped Mn1-xZnxFe2O4 nanoparticles, optical constants
Abstrak
This study aimed at investigating the effect of Zn2+ concentration on the optical constants of Mn1-xZnxFe2O4 nanoparticles. The nanoparticles have been synthesized by using the coprecipitation method at a temperature of 90oC. The molar concentration of Zn2+ in the system of Mn1-xZnxFe2O4 is varied of 0.4; 0.6; and 0.8. The optical constants of the nanoparticles have been characterized by using Specular Reflectance UV-Visible Spectrophotometer (SR UV-Vis). The results show that absorbance, transmittance, %reflectance, absorption coefficient, refractive index, extinction coefficient, optical gap energy, Urbach energy, and optical conductivity depend on the concentration of Zn2+. Increasing Zn2+ leads to increasing those optical constants due to quantum confinement effects. The Zn2+ concentration directly affects the microstructure of the nanoparticles. Hence, the optical constants also directly depend on the microstructure. The Mn1-xZnxFe2O4 nanoparticles also show the photoconductive property that turns it to be very sensitive to the radiation of electromagnetic waves. Therefore, the nanoparticle has a potential application to be an active material for a signal amplifier of the SPR based biosensor.
Referensi
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Y. Bao, B. Zhao, D. Hou, J. Liu, F. Wang, X. Wang dan T. Cui, “The Redshift of Surface Plasmon Resonance of Colloidal Gold Nanoparticles Induced by Pressure with Diamond Anvil Cell,” Journal of Applied Physics, vol. 115, no. 223503, pp. 1-6, 2014.
A. S. Kushwaha, A. Kumar, R. Kumar, M. Srivastava dan S. K. Srivastava, “Zinc Oxide, Gold and Graphene-Based Surface Plasmon Resonance (SPR) Biosensor for Detection of Pseudomonas Like Bacteria: A Comparative Study,” Optik, vol. xxxx, no. xxx, pp. xxx-xxx, 2018.
P. S. Menon, F. A. Said, G. S. Mei, M. A. Mohamed, A. R. Mdzain, S. Shaari dan B. Y. Majlis, “High Sensitivity Au-based Kretschmann Surface Plasmon Resonance Sensor for Urea Detection,” Sains Malaysia, vol. 48, no. 6, p. 1179–1185, 2019.
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M. S. Rahman, M. R. Hasan, K. A. Rikta dan M. S. Anower, “A Novel Graphene Coated Surface Plasmon Resonance Biosensor with Tungsten Disulfide (WS2) for Sensing DNA Hybridization,” Optical Materials, vol. 75, pp. 567-573, 2018.
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M. J. Akhtar dan M. Younas, “Structural and Transport Properties of Nanocrystalline MnFe2O4 Synthesized by Coprecipitation Method,” Solid State Sciences, vol. 14, pp. 1536-1542, 2012.
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J. Li, H. Yuan, G. Li, Y. Liu dan J. Leng, “Cation Distribution Dependence of Magnetic Properties of Sol–Gel Prepared,” Journal of Magnetism and Magnetic Materials, vol. 322, p. 3396–3400, 2010.
I. Ibrahim, I. O. Ali, T. M. Salama, A. A. Bahgat dan M. M. Mohamed, “Synthesis of Magnetically Recyclable Spinel Ferrite (MFe2O4, M = Zn, Co, Mn) Nanocrystals Engineered by Sol Gel-Hydrothermal Technology: High Catalytic Performances for Nitroarenes Reduction,” Applied Catalysis B: Environmental, vol. 181, p. 389–402, 2016.
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J. J. Vijaya, G. Sekaran dan M. Bououdina, “Effect of Cu2+ Doping on Structural, Morphological, Optical and Magnetic Properties of MnFe2O4 Particles/Sheets/Flakes-Like Nanostructures,” Ceramics International, vol. xxxx, no. xxx, pp. xxx-xxx, 2013.
M. A. Gabal dan S. S. Ata-Allah, “Concerning the Cation Distribution in MnFe2O4 Synthesized Through the Thermal Decomposition of Oxalates,” Journal of Physics and Chemistry of Solids, vol. 65, p. 995–1003, 2004.
E. R. Kumar, P. S. P. Reddy, G. S. Devi dan S. Sathiyaraj, “Structural, Dielectric and Gas Sensing Behavior of Mn Substituted Spinel MFe2O4 (M= Zn, Cu, Ni, and Co) Ferrite Nanoparticles,” Journal of Magnetism and Magnetic Materials, vol. 398, p. 281–288, 2016.
Q.-m. Wei, J.-b. Li, Y.-j. Chen dan Y.-s. Han, “Cation Distribution in NixMn1−xFe2O4 Ferrites,” Materials Chemistry and Physics, vol. 74, p. 340–343, 2002.
G. Mathubala, A. Manikandan, S. A. Antony dan P. Ramar, “Photocatalytic Degradation of Methylene Blue Dye and Magneto-optical Studies of Magnetically Recyclable Spinel NixMn1-xFe2O4 (x= 0.0 - 1.0) Nanoparticles,” Journal of Molecular Structure, vol. 1113, pp. 79-87, 2016.
L. L. Lang, J. Xu, Z. Z. Li, W. H. Qi, G. D. Tang, Z. F. Shang, X. Y. Zhang, L. Q. Wu dan L. C. Xue, “Study of the Magnetic Structure and the Cation Distributions in MnCo Spinel Ferrites,” Physica B, vol. 462, p. 47–53, 2015.
J. Giri, T. Sriharsha, S. Asthana, T. K. G. Rao, A. K. Nigam dan D. Bahadur, “Synthesis of Capped Nanosized Mn1-xZnxFe2O4 (x = 0 s.d 0.8) by Microwave Refluxing for Bio-medical Applications,” Journal of Magnetism and Magnetic Materials, vol. 293, p. 55–61, 2005.
H. Hejase, S. S. Hayek, Q. Shahnaz dan H. Yousef , “MnZnFe Nanoparticles for Self-controlled Magnetic Hyperthermia,” Journal of Magnetism and Magnetic Materials, vol. 324, p. 3620–3628, 2012.
M. Satalkar, N. Ghodke dan S. N. Kane, “Influence of High Temperature Sintering on the Structural and Magnetic Properties of Mn1-xZxFe2O4,” dalam Journal of Physics: Conference Series, 2014.
J. Xie, Y. Zhang, C. Yan, L. Song, S. Wen, F. Zang, G. Chen, Q. Ding, C. Yan dan N. Gu, “High-Performance PEGylated Mn-Zn Ferrite Nanocrystals as a Passive-Targeted Agent for Magnetically Induced Cancer Theranostics,” Biomaterials, vol. 35, pp. 9126-9136, 2014.
I. P. T. Indrayana, “Analisis Parameter Mikrostruktur Nanopartikel Mn1-xZnxFe2O4 Berdasarkan Pola Difraksi Sinar X,” Jurnal Sains dan Teknologi, vol. 8, no. 1, pp. 23-34, 2019.
I. P. T. Indrayana dan E. Suharyadi, “Crystallite Size-Lattice Strain Estimation and Optical Properties of Mn0.5Zn0.5Fe2O4 Nanoparticles,” dalam Journal of Physics: Conf. Series, 2018.
I. P. T. Indrayana, N. Siregar, E. Suharyadi, T. Kato dan S. Iwata, “The Calcination Temperature Dependence of Microstructural, Vibrational Spectra, and Magnetic Properties of Nanocrystalline Mn0.5Zn0.5Fe2O4,” dalam Journal of Physics: Conference Series, 2016.
M. Su, C. He, V. K. Sharma, M. A. Asi, D. Xia, X. Z. Li, H. Deng dan Y. Xiong, “Mesoporous Zinc Ferrite: Synthesis, Characterization, and Photocatalytic Activity with H2O2/Visible Light,” Journal of Hazardous Materials, vol. 211– 212, p. 95– 103, 2012.
A. Meidanchi, O. Akhavan, S. Khoei, A. A. Shokri, Z. Hajikarimi dan N. Khansari, “ZnFe2O4 Nanoparticles as Radiosensitizers in Radiotherapy of Human Prostate Cancer Cells,” Materials Science and Engineering C, vol. 46, p. 394–399, 2015.
R. M. Sebastian, S. Xavier dan M. EM, “Effect of Sintering Temperature on the Structural Magnetic and Electrical Properties of Zinc Ferrite Samples,” Journal of Nanomaterials & Molecular Nanotechnology, vol. 4, no. 2, 2015.
J. Zhang, J.-M. Song, H.-L. Niu, C.-J. Mao, S.-Y. Zhang dan Y.-H. Shen, “ZnFe2O4 Nanoparticles: Synthesis, Characterization, and Enhanced Gas Sensing Property for Acetone,” Sensors and Actuators B, vol. 221, p. 55–62, 2015.
A. Baykal, S. Güner dan A. Demir, “Synthesis and Magneto-optical Properties of Triethylene Glycol Stabilized Mn1-xZnxFe2O4 Nanoparticles,” Journal of Alloys and Compounds, vol. 619, p. 5–11, 2015.
H. Erdemi dan A. Baykal, “Dielectric Properties of Triethylene Glycol-stabilized Mn1-xZnxFe2O4 Nanoparticles,” Materials Chemistry and Physics, vol. xxx, pp. 1-12, 2015.
S. C dan S. C, “Structural, Optical Properties of Manganese–Zinc Ferrite,” International Journal of Recent Scientific Research, vol. 10, no. 3, pp. 31486-31490, 2019.
G. Vasuki dan T. Balu, “Systematic Investigations on the Effect of Divalent Metal Ions (Mg2+ and Zn2+) Substitution on Nanocrystalline Manganese Ferrites,” Journal of Nano and Electronic Physics, vol. 11, no. 1, pp. 1-5, 2019.
S. R. Patade, D. D. Andhare, P. B. Kharat, A. V. Humbe dan K. M. Jadhav, “Impacts of Crystallites on Enhancement of Bandgap of Mn1-xZnxFe2O4 (1 ≥ x ≥ 0) Nanospinels,” Chemical Physics Letters, vol. xxxx, no. xxx, pp. xxx-xxx, 2020.
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2020-08-12
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[1]
I. P. T. Indrayana dan R. Almi Putra, “Pengaruh Konsentrasi Doping Zn2+ Terhadap Nilai Konstanta Optik Nanopartikel Mn1-xZnxFe2O4 ”, hadron, vol. 2, no. 1, hlm. 5-15, Agu 2020.
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